ICP—MS同时测定聚合氯化铝中的Al2O3及5种元素含量的研究
收稿日期: 1999-12-20
网络出版日期: 2010-10-01
The determination of Al2O3 and 5 elements in poly aluminium chloride by inductively coupled plasma mass spectrometer method
Received date: 1999-12-20
Online published: 2010-10-01
研究结果表明:用ICP—MS可以同时测定聚合氯化铝中的Al2O3及As、Mn、Hg、Pb、Cd5种元素的含量。测试样品(100倍稀释固体聚合氯化铝)中Al2O3、As、Mn、Hg、Pb、Cd的测定结果分别为:0.30%、1.87μg/L、95.4μg/L、46.0ng/L、23.3μg/L、574ng/L;测定的准确度分别为930%、109%、944%、883%、980%、886%。ICP—MS法具有10-12~10-6级多元素同时分析、测定快速、样品前处理简单、干扰少、省事、省力等无可比拟的优点。
关键词: 电感耦合等离子体质谱; 聚合氯化铝; 无机高分子絮凝剂
农晋琦, 卢益新, 朱蓉 . ICP—MS同时测定聚合氯化铝中的Al2O3及5种元素含量的研究[J]. 工业水处理, 2000 , 20(2) : 35 -37 . DOI: 10.11894/1005-829x.2000.20(2).35
A method for the determination of Al2O3 and 5 elements Al 、As 、Mn 、Hg 、Pb 、Cd in poly aluminium chloride by inductively coupled plasma mass spectrometer (ICP —MS)has been established.They found Al2O3 and these 5 elements in polyaluminium chloride could be simultaneously determined by ICP —MS.The contents of Al2O3 and As 、Mn 、Hg 、Pb 、Cd in test sample (100 times dilution)are 0.30 %,1.87μg/ L,95.4μg/L,46.0 ng/L,23.3 μg/ L,574 ng/L respectively,and the accuracies of this test are 93.0 %,109 %,94.4 %,88.3 %,98.0 %,88.6 % respectively.
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