液相色谱质谱法快速测定水中痕量涕灭威和克百威
|
李利荣,张静,刘殿甲,吴宇峰,张肇元,王效国,张海波,许亮
|
Rapid determination of trace aldicarb and carbofuran in water by HPLC-MS/MS
|
Lirong Li,Jing Zhang,Dianjia Liu,Yufeng Wu,Zhaoyuan Zhang,Xiaoguo Wang,Haibo Zhang,Liang Xu
|
|
表3 涕灭威和克百威测定标准曲线
|
|
|
化合物 | | Cal-1 | Cal-2 | Cal-3 | Cal-4 | Cal-5 | Cal-6 | b | a | r | 甲萘威-D3 | 响应值 | 156 | 142 | 163 | 161 | 152 | 139 | — | — | — | 涕灭威 | 质量浓度/(μg·L-1) | 0.020 | 0.040 | 0.080 | 0.160 | 0.320 | 0.640 | 0.094 6 | 20.78 | 0.998 | 响应值 | 99.0 | 152 | 307 | 526 | 948 | 1 898 | 克百威 | 质量浓度/(μg·L-1) | 0.005 | 0.010 | 0.020 | 0.040 | 0.080 | 0.160 | 0.066 4 | 71.17 | 0.999 | 响应值 | 83.0 | 144 | 218 | 445 | 947 | 1 704 |
|
|
|