搅拌棒吸附萃取-LC-MS/MS测定二氯吡啶酸
施晓婷
Determination of clopyralid by liquid chromatography-mass spectrometry combined with stir bar sorptive extraction
Xiaoting Shi
表2
L
9
(3
4
)正交试验结果
序号
A
B
C
D
萃取率/%
1
1
1
1
1
89.1
2
1
2
2
2
84.2
3
1
3
3
3
88.0
4
2
1
2
3
95.1
5
2
2
3
1
84.6
6
2
3
1
2
77.4
7
3
1
3
2
89.6
8
3
2
1
3
90.7
9
3
3
2
1
75.7
K
1
2.61
2.74
2.57
2.49
K
2
2.57
2.60
2.55
2.51
K
3
2.56
2.41
2.62
2.74
R
0.02
0.33
0.07
0.24
因素主次
B
>
D
>
C
>
A
最佳组合
A
1
B
1
C
3
D
3