For the increasingly elevated electroplating wastewater discharge standard in Tai Lake area, coagulantmicrofiltration membrane filtration combined process has been used for removing copper and nickel from electroplating wastewater. From the angle of engineering application,the influential factors of FeSO₄ coagulant -microfiltration membrane combined process are studied and discussed,and the most optimum running parameters are confirmed,and its practicability is investigated. The concentration of Cu²⁺ in electroplating wastewater sample is 57.6 mg/L,and that of Ni²⁺is 42.0 mg/L. The concentration of copper and nickel in outflow are changed to 0.15 mg/L and 0.87 mg/L respectively,after treated by FeSO₄ coagulant and PVDF microfiltration membrane. They are both lower than the first class of Wastewater Comprehensive Discharge Standard,and the process has relatively strong economic applicability.