工业水处理 ›› 2011, Vol. 31 ›› Issue (8): 52-54. doi: 10.11894/1005-829x.2011.(31).8.52

• 试验研究 • 上一篇    下一篇

PW/MCM-41光催化性能研究

黄艳芹1, 程玉良2, 周建伟3   

  1. 1. 新乡学院化学与化工学院, 河南新乡 453003;
    2. 新乡学院生命科学与技术系, 河南新乡 453003;
    3. 新乡学院能源与燃料研究所, 河南新乡 453003
  • 收稿日期:2011-04-21 修回日期:2011-04-21 出版日期:2011-08-20 发布日期:2011-08-29
  • 作者简介:黄艳芹(1966- ),2007 年毕业于河南师范大学,硕士,副教授,从事应用化学研究。电话:13937359854,E-mail: hyq200405@sohu.com。
  • 基金资助:

    河南省重点科技攻关项目(092102310184);河南省教育厅2008年度自然科学研究计划项目(2008C480002)

Study on photocatalytic capacity of PW/MCM-41

Huang Yanqin1, Cheng Yuliang2, Zhou Jianwei3   

  1. 1. Department of Chemistry and Chemical Engineering, Xinxiang University, Xinxiang 453003, China;
    2. Department of Life Sciences and Technology, Xinxiang University, Xinxiang 453003, China;
    3. Institute of Energy & Fuel, Xinxiang University, Xinxiang 453003, China
  • Received:2011-04-21 Revised:2011-04-21 Online:2011-08-20 Published:2011-08-29

摘要:

以浸渍法制备了负载型光催化剂PW/MCM-41,并对催化剂进行了表征,考察了催化剂在光催化模拟染料废水亚甲基蓝(MB)溶液降解反应中的催化活性。实验结果表明:催化剂负载量为30%、催化剂投加质量浓度为3.0 g/L、MB溶液的初始质量浓度为10 mg/L、pH=5、光照时间100 min时,对亚甲基蓝降解率可达91%以上,且催化剂可重复使用。

关键词: 磷钨酸, MCM-41分子筛, 光催化降解, 亚甲基蓝

Abstract:

PW/MCM-41 has been prepared and characterized by immersion method. The catalytic activity of the photocatalyst in the degradation reaction of photocatalytic simulated dyeing wastewater methylene blue(MB)solution is investigated. The results show that when the catalyst charge number is 30%,mass concentration of catalyst dosage 3.0 g/L,the concentration of methylene blue 10 mg/L,pH=5,and light application time 100 min,the photocatalytic degradation rate is as high as 91% over. Furthermore,the catalyst could be used repeatedly.

Key words: phosphotungstic acid, MCM-41 molecular sieve, photocatalytic degradation, methylene blue

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