工业水处理 ›› 2009, Vol. 29 ›› Issue (4): 76-78. doi: 10.11894/1005-829x.2009.29(25).76

• 分析与监测 • 上一篇    下一篇

荧光法测定油田采出水中示踪剂的含量

吴红军1, 王丽艳1, 王宝辉1, 刘刚2, 于家涛3, 王德蛟4   

  1. 1. 大庆石油学院化学化工学院, 黑龙江大庆 163318;
    2. 天津大港油田, 天津 300280;
    3. 大庆石化分公司, 黑龙江大庆 163714;
    4. 哈尔滨科学技术职业学院(二校区), 黑龙江哈尔滨 150001
  • 出版日期:2009-04-20 发布日期:2010-10-01
  • 作者简介:吴红军(1979- ),大庆石油学院,在读博士,讲师,主要研究方向为: 新能源与环境化学。电话:0459 - 6503331,E-mail:hjwu1979@163.com。

Determination of the tracer in oilfield produced water by fluorometry

Wu Hongjun1, Wang Liyan1, Wang Baohui1, Liu Gang2, Yu Jiatao3, Wang Dejiao4   

  1. 1. College of Chemistry & Chemical Engineering, Daqing Petroleum Institute, Daqing 163318, China;
    2. Tianjin Dagang Oilfield, Tianjin 300280, China;
    3. Daqing Petrochemical Company, Daqing 163714, China;
    4. Harbin Science & Technology Professional Institute(2nd Campus), Harbin 150001, China
  • Online:2009-04-20 Published:2010-10-01

摘要:

对示踪剂荧光素性质进行考察,通过对待测水样用KOH调节pH至8,利用荧光法测定油田采出水中示踪剂的含量。该方法简便、快速且灵敏度高,测定值的相对标准偏差在0.167%以内,加标回收率为96.73%~104.00%。

关键词: 示踪剂, 荧光素, 荧光法, 油田采出水

Abstract:

The luminescent properties and stability of fluorescein which is used as a tracer in oilfield produced water have been investigated.The pH of the water samples to be tested should be adjusted to 8 with KOH.The tracer content in oilfield produced water is determined by fluorometry.This method is simple,convenient,and fast,having high sensibility.The relative standard deviation of this method is within 0.167%,and the indexed recovery rates are 96.73%-104.00%.

Key words: tracer, fluorescein, fluorometry, oilfield produced water

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