INDUSTRIAL WATER TREATMENT ›› 2002, Vol. 22 ›› Issue (10): 38-39. doi: 10.11894/1005-829x.2002.22(10).38

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Determination of the concentration of lead ions in wastewater by chelatometric titration

LI Fangwen, WEI Xianxun, LI Caiting, ZHANG Dejian, ZHAI Yunbo   

  1. Department of Environmental Science and Engineering, Hunan University, Changsha 410082, China
  • Received:2002-06-28 Online:2002-10-20 Published:2010-10-01

络合滴定法测定废水中铅离子的浓度

李方文, 魏先勋, 李彩亭, 张德见, 翟云波   

  1. 湖南大学环境科学与工程系, 湖南长沙 410082
  • 作者简介:李方文(1970- ),1993年毕业于湖南高等医学专科学校工业卫生与环境卫生专业.讲师,现为湖南大学在读硕士研究生.E-mail:lifangweng1@sohu.com.电话:0731- 8821462.

Abstract:

A new method of determining the concentration of lead ions.This methods makes up the limitation which the common ways (e.g.dithizone colorimetry and atomic absorption spectrophotometry)have if virudent poison KCN is used, the standard curve is protracted, the operation process is too complicated, and is only suitable for the determination of matter with low concentration.The operation process of the new method is simple and the determination result is accurate (the relative error is 0.01 %and the relative standard deflectivity is 0.41 %).It is suitable for the determination of lead with high concentration.

Key words: chelatometric titration, wastewater, lead ions

摘要:

介绍了一种测定铅离子浓度的新方法,克服了常用方法 (双硫腙比色法、原子吸收分光光度法 )要使用剧毒物质KCN、绘制标准曲线、操作过程复杂及仅适合低浓度测定等局限性。该方法测定过程简单,测定结果准确(相对误差为 0.0 18%,相对标准偏差为 0.4 1% ),适合高浓度铅的测定

关键词: 络合滴定, 废水, 铅离子

CLC Number: