工业水处理 ›› 2014, Vol. 34 ›› Issue (3): 68-70. doi: 10.11894/1005-829x.2014.34(3).068

• 试验研究 • 上一篇    下一篇

Fe3O4@TiO2-膨胀石墨的制备及其光催化性能研究

于秀娟1,2, 李显伟1, 万家峰1,2, 程修文1   

  1. 1. 黑龙江大学环境科学与工程系, 黑龙江哈尔滨 150080;
    2. 黑龙江省普通高等学校高效转化的化工过程与技术重点实验室, 黑龙江哈尔滨 150080
  • 收稿日期:2013-11-18 出版日期:2014-03-20 发布日期:2014-03-21
  • 作者简介:于秀娟(1965-),教授,博士。电话:18345038403,E-mail:hljyuxiujuan@126.com。

Preparation and photocatalytic activity of Fe3O4@TiO2-expanded graphite

Yu Xiujuan1,2, Li Xianwei1, Wan Jiafeng1,2, Cheng Xiuwen1   

  1. 1. Department of Environmental Science and Engineering, Heilongjiang University, Harbin 150080, China;
    2. Key Laboratory of Chemical Engineering Process & Technology for High-efficiency Conversion, Ordinary College of Heilongjiang Province, Harbin 150080, China
  • Received:2013-11-18 Online:2014-03-20 Published:2014-03-21

摘要:

制备了核壳式Fe3O4@TiO2-膨胀石墨光催化剂,考察了其吸附及光催化性能。实验结果表明:锐钛矿型TiO2对Fe3O4进行了有效包覆,并均匀地沉积在膨胀石墨的表面及沟壑中,制备的样品具有超顺磁性。核壳式改性Fe3O4@TiO2-膨胀石墨的比饱和磁化强度为28.3 emu/g,对苯酚的吸附率可达20.1%,降解率为72.1%。

关键词: 四氧化三铁, 二氧化钛, 膨胀石墨, 光催化活性

Abstract:

The core-shell particle Fe3O4@TiO2-expanded graphite has successfully been prepared. The adsorption and photo-catalytic capacities of it are investigated. The results show that the Fe3O4 particles are coated with anatase titanium dioxide effectively and deposited equally on the surface and gully of the prepared composite material,showing super paramagnetic characteristics. The saturation and magnetization strength of the modified core-shell particle Fe3O4@TiO2-expanded graphite is 28.3 emu/g,the adsorption rate for phenol can reach 20.1%,and the degradation rate of phenol 72.1%.

Key words: Fe3O4, TiO2, expanded graphite, photocatalytic activity

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